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Acid soak bath design

08/06/2008 11:12 AM

I've been asked to design a cleaning system that will comprise a holding tank of sulfuric acid at 95% concentration at 60 degrees celcius. The parts will be loaded into the wash tank after which the acid will be pumped up to a known level after which these parts will simple soak for 20 mins. The acid is then allowed to drain back into the holding tank after which the tank will again fill with de-ionised water at 50 degrees celcius for another 20 minutes before being put to drain. This is the basic process. The parts will then go onto ultrasonic cleaning etc. My concerns are the actual materials I should use, not only for the holding tank, but also for the wash tank itself, piping and pumps etc. I am also of the opinion that after every cycle there should be a drying cycle to remove any water residue to avoid cross contamination. Any help anyone please??

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Guru
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#1

Re: Acid soak bath design

08/06/2008 11:44 AM

What are the parts made of? 95% sulphuric acid at 60degC is quite aggressive, and it gets worse if water is brought near it!

PVDF is a popular material for pipework.

http://www.coleparmer.co.uk/techinfo/ChemComp.asp

Sulphuric acid has a high heat-of-dilution. Then, everyone knows to add acid to water and not water to acid, surely?

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#2
In reply to #1

Re: Acid soak bath design

08/06/2008 11:56 AM

...don't know, but this is a repeat set up. so I'm not really concerned. I've been given a process spec, but comments such as "supplier to advise" scare me a bit!! I've considered constructing the whole thing from PVDF, as I note that any of the more available stainless steels degenerate with this stuff at elevated temps. by incorporating a hot air drying cycle after de-i soaking, I'm hoping to reduce,eliminate the cross contamination problem. Thanks for your coments

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Guru
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#3
In reply to #2

Re: Acid soak bath design

08/06/2008 11:58 AM

If it's a repeat set-up, why not copy the original set-up?

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#4
In reply to #1

Re: Acid soak bath design

08/06/2008 12:16 PM

.....the acid is t be drained back into it's holding tank before the water is added. There should only be a residual amout of acid in the tank when the water is added. I understand that this is how the process works in the UK. This system is a new start up in China and is, I am told simply a repeat system. Maybe I need to go and view the existing system.

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Guru
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#5
In reply to #4

Re: Acid soak bath design

08/07/2008 3:32 AM

<...Maybe.....go and view the existing system.....>

Always highly recommended. There is often no need to reinvent the proverbial wheel.

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#6
In reply to #5

Re: Acid soak bath design

08/07/2008 11:06 AM

Quite so - all too often what is reinvented is the flat tire. Viewing what's to be replicated can sometimes point up errors, oversights, and misfires!

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