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Join Date: Sep 2011
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Production of Activated Carbon from Coconut Shell in Lab

09/19/2011 5:20 AM

Hi, I am student of last year of chemical engineering in India. I chose project of production of activated carbon from coconut shell. I review literature and found that 1st step is crushing of shell then it will converted to powder form. Then powder will mix with H3PO4, next step will be heating of mixture in dryer up to 850c. Finally activated carbon is produced as per literature.

Is it possible in lab (Suggest equipment required for whole procedure) and how can I check whether activated carbon is produced or ash is produced?

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Guru

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#1

Re: production of activated carbon from coconut shell in lab

09/19/2011 5:29 AM

1. Big honkin' hammer to beat the crap outa the shells.

2. Metal bowl to hold the powdered shells and H3PO4

3. Fire to heat it up.

If the product burns, it's charcoal. If it doesn't, it's ash.

Do your own homework!

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Guru

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#2

Re: Production of Activated Carbon from Coconut Shell in Lab

09/19/2011 11:48 AM

Drying somewhat is different than burning. It's just like cooking the shell till the pure Carbon remains, bone dry. That's the way carbon is activated.

As you know combustibles is Carbon & Hydrogen content CnHm, for solids n>m, liquids could be n~=m, gaseous n<m.

Exposing coconut shell to 850 deg C without burning gets rid of H & H2O(lighter constituents evaporates from heavier carbon, uncombustibles are always there, its the ash once it burned)

And by its nature (dry & Carbon-unstable-attractable to oxides) its what you call "activated carbon"

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Guru
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#3

Re: Production of Activated Carbon from Coconut Shell in Lab

09/19/2011 12:24 PM

You have to bake the mixture in an oxygen free atmosphere to form activated carbon, otherwise it will burn to form ash instead.

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Guru
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#4

Re: Production of Activated Carbon from Coconut Shell in Lab

09/19/2011 10:52 PM

The process of producing charcoal will also produce some gases which must be vented to outdoors, and open flames are commonly produced when volatiles in the material catch fire, after other gases, water vapour etcetera is all gone. Unless you have specialized equipment to handle flammable gases and flames, you should not attempt to do this indoors in the lab.

There's lots of video and instructional material for small scale production of charcoal from wood online - I've never seen one that is done indoors, and the same seems to apply to making activated charcoal from coconut shell. Gases released in the process include methane, carbon dioxide and organic volatiles/vapours.

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