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Measuring Water Content in Carbon Black-Water Mixtures

02/08/2008 7:43 AM

Are there any commercial devices for measuring water content in relatively dry mixes of carbon black powder and water.

Michael Binder

Applied Research

binder428@yahoo.com

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#1

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/08/2008 10:59 AM

Yes, for most granular or powder materials that have a high melting point.

The standard way of measuring their moisture content is to place a sample on a precision weighing balance and place an infrared heater over the sample...

As the moisture is driven out of the sample the weight decreases slowly and then starts to level off as the moisture is reduced to almost zero. From the original weight and the weight loss the moisture content can esily be determined.

These moisture meters are readily available, I think they're called infrared moisture analysers or something....

Hope that helps - John.

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#2

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/08/2008 2:09 PM

Place a sample in an oven and dry it. Cool the sample in a sealed container. Weight differences between the dried sample and an other sample should give water content.

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#3

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/09/2008 9:48 AM

Yes, commercial devices are available, but I dont know current manufacturers.

Back in the mid 1960s, we used a device (in the food industry at Corn Products Research) that basically consisted of a heat lamp shining on a weigh scale to make the measurement. The sample was placed onhing similar could be used for carbon black. the scale and zeroed for tare. The light shown on the sample and the weight was measured automatically by weight difference when the equilibrium was reached. I assume somet

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#4

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/10/2008 6:09 AM

Humidity measurement of dry mixtures is sometimes done with simple and cheap radar equipment where the frequency is correlated to the resonance freq of H2O. Vou have two chambers, one for measurement and one for reference, both radiated by the same source. So differences in intensity are compensated by making a relational evaluation after calibrating the system with a known content of humidity.

This is used par example for determining the water contents of grain before it is milled.


Regards Uwe

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#5

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/11/2008 8:24 AM

When I worked at a steel mill, we had a moisture guage that measured the percent

moisture in the Coke (almost pure carbon) that was in a weigh hopper to determine how much coke was charged, and how much water was in there.

This guage used a nuclear source and measured the backscatter.

That was 6 years ago. I am sure they are still using this at what used to be the

Bethlehem Steel, Burns harbor plant.

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#6

Re: Measuring Water Content in Carbon Black-Water Mixtures

02/27/2008 10:03 AM

Normally a drying scale is used; at our lab (at a carbon black manufacturing plant) we use a Mettler drying scale that uses a halogen lamp. The water content is expressed as a weight loss percentage.

See http://nl.mt.com/mt/filters/products-applications_laboratoriumwegen_halogeen-vochtanalyse/Moisture_Analyzer_0x000010083f6eb48c40005a4b.jsp (we use the left one)

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#7
In reply to #6

Re: Measuring Water Content in Carbon Black-Water Mixtures

08/25/2010 11:07 PM

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Carbon Black - Grade N220

PropertyASTMMINMAX
Iodine No. mg/gD1510116.0126.0
Oil Absorption, cc/100gD2414108.0120.0
Toluene Discolouration, %D16188.0-
Heat Loss, %D1509-2.0
Tint Strength vs IRB 3#D3265110.0125.0
Ash, %D1506-0.8
325# Sieve Residue,%D1514-0.100
Density, lb/cu ftD151320.024.0
Fines 5 min, %D1508-8.0
300% Modulus, vs IRB6 MpaD412-0.702.55

Carbon Black - Grade N330

PropertyASTMMINMAX
Iodine No. mg/gD151077.088.0
Oil Absorption, cc/100gD241495.0105.0
Toluene Discolouration, %D161880-
Heat Loss, %D1509-2.0
Tint Strength vs IRB 3#D326598.0108.0
Ash, %D1506-0.8
325# Sieve Residue,%D1514-0.100
Density, lb/cu ftD151321.525.0
Fines 5 min, %D1508-5.0
Fines 20 min, %D1508-8.0
300% Modulus, vs IRB6 MpaD4120.142.90

Carbon Black - Grade N550

PropertyASTMMINMAX
Iodine No. mg/gD151038.048.0
Oil Absorption, cc/100gD2414116.0126.0
Toluene Discolouration, %D161880-
Heat Loss, %D1509-2.0
Ash, %D1506-0.8
325# Sieve Residue,%D1514-0.100
Density, lb/cu ftD151320.024.0
Fines 5 min, %D1508-8.0
Fines 20 min, %D1508-12.0
300% Modulus, vs IRB6 MpaD4120.303.10

Carbon Black - Grade N660

PropertyASTMMINMAX
Iodine No. mg/gD151031.041.0
Oil Absorption, cc/100gD241485.095.0
Toluene Discolouration, %D161880-
Heat Loss, %D1509-2.0
Ash, %D1506-0.8
325# Sieve Residue,%D1514-0.100
Density, lb/cu ftD151324.028.0
Fines 5 min, %D1508-5.0
Fines 20 min, %D1508-8.0
Pellet Crush Strength, avg gD33131050
Pellet Crush Strength, max gD3313-60
300% Modulus, vs IRB6 MpaD412-1.501.30

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