Details of problem faced in plasma nitriding as below ---
1 ) Plasma takes place only below a pressure of one torr . As per practice the plasma nitriding is suppose to be done at around five torr.
2) Case depth achieved is about 20-30 micron only in 12 hrs nitriding cycle.
3) How to measure temperature in plasma system accurately. We use R.T.D. sensors.
4) We are using power supply of the following specifications.
|
SPECIFICATIONS FOR 60 KW POWER SUPPLY SYSTEM |
|
INPUT |
|
Nominal Voltage 415 V AC, (+ 10 % to – 10%) Three Phase & N |
|
Nominal Frequency 50 Hz. (+/- 10%) |
|
RECTIFIER |
|
Type Full Wave |
|
OUTPUT |
|
Power Capacity 60 KW |
|
Nominal Voltage 0 to 1200 V, Adjustable through 10 turn pot. With dial |
|
Frequency 1kHz to 6 kHz Variable |
|
Duty cycle 10% to 95% |
|
Waveform Duty cycle controlled chopped DC output with variable frequency. |
|
EFFICIENCY At full load |
|
Overall Efficiency (AC to AC) > 90% at 100% Load |
|
ENVIRONMENTAL |
|
Acoustic Noise Level <64 db @1.5 Meter |
|
Ambient Temperature 0 to 40 Deg C |
|
Storage Temperature -10 to 70 Deg C |
|
Humidity Upto 95% RH, Non Condensing |
|
Altitude < 1000 Mtrs. Above Sea Level ( without derating) |
|
PHYSICAL |
|
Enclosure Protection Grade IP – 41 |
|
Cooling Forced Air |
|
Colour Siemens Gray |
|
Cable Entry Bottom |
|
Dimensions (in mm) Tentative W D H |
|
800 800 1770 |
|
Weight –Tentative 400 Kg |
|
METERING |
|
DC Voltage (digital) Output Current Output Frequency |
|
Output Wattage |
|
INDICATIONS |
|
LED Indications Control Supply OK Rectifier over voltage |
|
PROTECTIONS |
|
Input Contactor |
|
Input Single Phasing / phase |
|
reversal |
|
Rectifier Over voltage |
|
High speed over current |
|
Over temperature |
|
Arc suppression |
|
Output Overload |
|
Output Short |
|
Circuit |
|
¥ Alarms are provided for all important protections. |
|
TESTING STANDARDS |
|
IEC 62040 - PART III |
5) The other parameters used during the trials are as below
During sputtering Gas Flow
H2 – 100 ml/min.
Ar - 100ml/min.
During nitriding
N2- 10ml/min.
H2- 90ml/min.
6) Material details
Composition W.P.S. EN41
HDS
C + CR + MO + W C -1.25 to 1.55% 1.5% CR/AL/MO
(0.36.4%) (4.80 to 5.2%) (1.2 to 1.6%) (8.0%) CR- 11 to 12 %
M - .5 to 1.0 %
V - .6 to 1.0%
Power Used Details
Sputtering Nitriding
Voltage – Max 1000V o 1100VDC 650 to 900
Current – 30A to 40 Amps 40 to 45 Amps
Frequency – 1KH2 1KH2
Temperature – 4500Celcius 450± 300 Celcius