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Participant

Join Date: May 2008
Location: Nashik ,Maharashtra, India
Posts: 2

Plasma Nitriding System

07/31/2008 2:54 AM

Details of problem faced in plasma nitriding as below ---

1 ) Plasma takes place only below a pressure of one torr . As per practice the plasma nitriding is suppose to be done at around five torr.

2) Case depth achieved is about 20-30 micron only in 12 hrs nitriding cycle.

3) How to measure temperature in plasma system accurately. We use R.T.D. sensors.

4) We are using power supply of the following specifications.

SPECIFICATIONS FOR 60 KW POWER SUPPLY SYSTEM

INPUT

Nominal Voltage 415 V AC, (+ 10 % to – 10%) Three Phase & N
Nominal Frequency 50 Hz. (+/- 10%)

RECTIFIER

Type Full Wave

OUTPUT

Power Capacity 60 KW
Nominal Voltage 0 to 1200 V, Adjustable through 10 turn pot. With dial
Frequency 1kHz to 6 kHz Variable
Duty cycle 10% to 95%
Waveform Duty cycle controlled chopped DC output with variable frequency.

EFFICIENCY At full load

Overall Efficiency (AC to AC) > 90% at 100% Load

ENVIRONMENTAL

Acoustic Noise Level <64 db @1.5 Meter
Ambient Temperature 0 to 40 Deg C
Storage Temperature -10 to 70 Deg C
Humidity Upto 95% RH, Non Condensing
Altitude < 1000 Mtrs. Above Sea Level ( without derating)

PHYSICAL

Enclosure Protection Grade IP – 41
Cooling Forced Air
Colour Siemens Gray
Cable Entry Bottom
Dimensions (in mm) Tentative W D H
800 800 1770
Weight –Tentative 400 Kg

METERING

�� DC Voltage (digital) �� Output Current �� Output Frequency
�� Output Wattage

INDICATIONS

LED Indications �� Control Supply OK �� Rectifier over voltage

PROTECTIONS

�� Input Contactor
�� Input Single Phasing / phase
reversal
�� Rectifier Over voltage
�� High speed over current
�� Over temperature
�� Arc suppression
�� Output Overload
�� Output Short
Circuit
¥ Alarms are provided for all important protections.

TESTING STANDARDS

IEC 62040 - PART III

5) The other parameters used during the trials are as below

During sputtering Gas Flow

H2 – 100 ml/min.

Ar - 100ml/min.

During nitriding

N2- 10ml/min.

H2- 90ml/min.

6) Material details

Composition W.P.S. EN41

HDS

C + CR + MO + W C -1.25 to 1.55% 1.5% CR/AL/MO

(0.36.4%) (4.80 to 5.2%) (1.2 to 1.6%) (8.0%) CR- 11 to 12 %

M - .5 to 1.0 %

V - .6 to 1.0%

Power Used Details

Sputtering Nitriding

Voltage – Max 1000V o 1100VDC 650 to 900

Current – 30A to 40 Amps 40 to 45 Amps

Frequency – 1KH2 1KH2

Temperature – 4500Celcius 450± 300 Celcius

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Guru

Join Date: Dec 2006
Location: Germany 49° 26' N, 7° 46' O
Posts: 1950
Good Answers: 109
#1

Re: Plasma Nitriding System

08/01/2008 3:42 AM

Hi,

are you sure with the frequency "1kHz to 6 kHz Variable"?

The Al has electrically insulating nitrides, I am not sure with Cr and Mo and ?W.

If insulating layers are formed then current is decaying very fast after polarity change.

If you make a measurement of the waveforms of voltage and current you will see this.

I would expect frequency to be 13MHz or above to work with insulating surfaces..

2. Depth of nitriding is not achieved by voltage and time but by diffusion of Nitrogen with temperature. Run a test with temperature and no voltage, is this working too? Run a test at higher temperature is this giving better depth?

3. There is nothing like a temperature but there is an electron velocity = temperature and a distribution of ion velocities = ion temperature.

Have a look into the old but good book from "Chen: Glow Discharge Processes".

Report your progress please!

RHABE

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