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Components of a Wetted Wall Column Setup

06/03/2011 9:04 AM

Say for instance you want to perform absorption using a wetted wall column with the solute gas being made to pass upward through the column and the liquid absorbent film falling down (counter current).

Is it really needed that a vacuum be attached to the gas outlet? I'm just beginning to take lectures on unit operations on mass transfer this term so I have no hands-on experience on WWC's yet.

This will be used in my thesis and I need to have this fabricated. The fabricator stressed that the gas may be pulled down by the flow of the liquid, keeping it from rising to the top. Then popped the question about whether I considered theories concerning climbing film columns and the calandria method.

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#1

Re: Components of a Wetted Wall Column Setup

06/03/2011 11:03 AM

There is nothing to stop the gas from going down other than a small pressure difference between the bottom and the top that keeps the gas flowing upwards, so there may well be an underflow/overflow weir arrangement at the bottom of the column to form a vapour seal. Such a device lets the liquid out while stopping the gas.

Without a more detailed description of the unit it is difficult to add anything else, apart from, why a wetted wall column when a packed column would do the same general job in a smaller volume (albeit with a greater gas pressure drop to consider)?

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#2
In reply to #1

Re: Components of a Wetted Wall Column Setup

06/03/2011 12:44 PM

"why a wetted wall column"?

Because that's is homework assignment.

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#4
In reply to #2

Re: Components of a Wetted Wall Column Setup

06/04/2011 12:33 AM

why you say? Frankly i couldn't think of anything else that could simulate something that is closely similar to those columns used in industries wherein you can also apply conduction (annular water jacket) to reduce the temperature while keeping the components of the absorbent liquid from volatilizing. Furthermore, i'm thinking that this can be further used to studying the kinetics of the absorption reaction in a simpler way. So far i haven't seen any other papers related to my topic of study that uses packed columns. Probably it's due to the lack of definite or accurate kinetic data.

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#5
In reply to #1

Re: Components of a Wetted Wall Column Setup

06/04/2011 12:43 AM

So that works even for a column height of 3.6 ft? (sorry for not stating the specs)

As for choosing this kind of column above anything else... i stated it on my reply to the next post.

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#3

Re: Components of a Wetted Wall Column Setup

06/03/2011 3:03 PM

I agree that this sounds like a mangled homework assignment. However as the OP stated that this is a facet of a lecture that puzzles them and the accompanying information seems mangled. I tend to believe the OP that this is not a homework question (lighten up Lyn ).

I suspect that your vacuum pump is at least first used to evacuate the previous gas column to a significantly high degree so that the gas column will be dominated by your added gas. Now depending on the critical Physics and Chemistry that happens in this column you might have a necessity to maintain a certain pressure (particle density) and average directional velocity (up) so that to maintain this flow you must pump down the travelling gas that reaches the top of the gas column. Come to think of it there may also be value in the gas being a known purity at the beginning of it's travel so that at the vacuum pump extraction it will have been exposed to the wet fluid for a known fixed period of time.

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#6

Re: Components of a Wetted Wall Column Setup

06/04/2011 12:49 AM

I'm sorry if this looks like i had to abuse this forum to do this thesis which appears like a mangled homework. But i find difficulty having to do this since i have to study alone ahead of the lectures stated in the curriculum. Simply put I'm a novice and this is all i can come up with the research me and my thesis mates did ourselves.

I am grateful for hearing your opinions.

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#7
In reply to #6

Re: Components of a Wetted Wall Column Setup

06/04/2011 4:04 AM

Any news from the implementation? I guess you need vacuum so the fluid evaporates below 100°C. Which is necessary in cases you don't have that much sunshine. What is the apparatus behind that evaporating unit?

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#8
In reply to #7

Re: Components of a Wetted Wall Column Setup

06/04/2011 6:17 AM

Um sorry i think you misunderstood me there. The fluid should NOT evaporate. That's why i had a water jacket made at the outer side of the column to keep the temperature low. My problem is whether the gas will be able to make it through the column upwards against the downward flow of the fluid. In fact I am wondering myself whether that really happens so i'm here to seek advice from those who already had experience in doing experiments regarding wetted wall columns. However, this is not a case of humidification but the opposite which is absorption.

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