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Speaking of Precision

Speaking of Precision is a knowledge preservation and thought leadership blog covering the precision machining industry, its materials and services. With over 36 years of hands on experience in steelmaking, manufacturing, quality, and management, Miles Free (Milo) Director of Industry Research and Technology at PMPA helps answer "How?" "With what?" and occasionally "Really?"

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Dimensional Contraction of 17-4 PH Stainless Steel

Posted February 29, 2012 9:00 AM by Milo

The mechanical properties of 17-4 PH must be fully developed by age hardening from Condition A in order to reduce risk of failure and to take full advantage of the material's capabilities.

Dodge Viper Throttles made by Bouchillon feature 17-4 PH shafts

17-4 PH is a martensitic precipitation hardening (age hardening) stainless steel that can provide both high strength and excellent corrosion resistance.

In the annealed (solution treated condition- Condition A) the density of this material is 0.280 lb/in^3.

H 900 density is 0.282 lb/in^3.

H 1075 density is 0.283 lb/in^3.

H 1150 density is 0.284 lb/in^3.

These changes in density values show that this alloy undergoes a volume contraction when it is hardened. This volume contraction is predictable and must be taken into account if you are trying to hold close tolerances.

The contraction factor for the change from Condition A to Condition H 900 ranges from 0.0004 to 0.0006 in/in or (mm/mm).

Hardening from Condition A to Condition H 1150 contracts in the range of approximately 0.0009 to 0.0012 in/ in or (mm/mm).

Here are three reasons to NOT use 17-4 PH in the Condition A state:

  • The structure is untempered martensite. This means low fracture toughness.
  • The structure is untempered martensite. This means low ductility.
  • Without age hardening, this material is more susceptible to stress corrosion cracking.

17-4 PH martensitic stainless steel can achieve high strength and superior corrosion resistance when precipitation hardened from Condition A to one of the Condition H tempers. It is used in many high performance applications made by our industry including valve parts for oilfield and chemical plant use; Fittings for aerospace and aircraft use; Jet engine componentry; Fasteners; Shafts for pumps; Dodge Viper carburetors! Many others.

In applications where high performance is mandatory, it is also mandatory to follow needed thermal treatment practices to assure the development of the full range of material properties that the material can provide.

For the savvy machinist, that also means understanding the potential effect of that thermal treatment on final size due to dimensional contraction when hardened.

Thanks to Bouchillon for the throttle photo.

Material on Dimensional Contraction was taken from Schmolz + Bickenbach 17-4 Datasheet.

Density and European Equivalency data from Rolled Alloys data sheet.

European designation note: Officially 17-4 PH is designated as UNS S17400. It is the US available nominal equivalent to DIN 1.4548, X5CrNiCuNb 17-4-4

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#1

Re: Dimensional Contraction of 17-4 PH Stainless Steel

02/29/2012 2:39 PM

This is kind of confusing.

First they say:

In the annealed (solution treated condition- Condition A) the density of this material is 0.280 lb/in^3.

Then:

The contraction factor for the change from Condition A to Condition H 900 ranges from 0.0004 to 0.0006 in/in or (mm/mm).

Hardening from Condition A to Condition H 1150 contracts in the range of approximately 0.0009 to 0.0012 in/ in or (mm/mm).

This makes it sound like it could be unannealed, which makes no sense. Is the Condition A, the treated material or are the H series the treated material? (my paragraph - I can't seem to format all of a sudden).

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#2
In reply to #1

Re: Dimensional Contraction of 17-4 PH Stainless Steel

02/29/2012 3:32 PM

The solution treated condition is Condition A. It is also called solution annealled.

Regardless, it is untempered martensite as the predominate icrostructure. Tempering to higher temperatures (the numbers after the condition H designator- ie 900 or 1150) followed by cooling in air results in the precipitation of a new copper precipitate phase. I also believe that some tempering of the martensite is going on, as well as the possible formation of reverted austenite. I have seen a paper, though, that claims the tempering of martensite during aging is insignificant in this steel...

The point is that whatever happens, these changes result in a tougher product and one that is more corrosion resistant.

Some suppliers do a double age, but that is beyond the scope of my experience.

I wrote this, thanks for your feedback on readability.

Milo

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#3

Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/01/2012 1:40 PM

Your math is wrong. 1.000-(.280/.282)^.3333=.002 not ".0004 to .0006". Similarly, 1.000-(.280/.284)^.3333=.004 not ".0009 to .0012".

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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/01/2012 1:55 PM

Nothing wrong with my math, and by the way these are published figures, credited to Schmolz + Bickenbach in my post.

Your calculations are using density for cubic inch;

The shrinkage factors are in inches per inch.

The density factors were given as experimental correlation to illustrate and support why the contraction.

Have a nice day.

Milo

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#5
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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/01/2012 2:55 PM

You will note that I used the third root of the density ratio to calculate linear contraction. The guys you are quoting apparently used the fourteenth root, and no one checked. Technical publications are often copy edited by English majors, because some engineers can't right to good, but some else should check the math.

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#6

Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/01/2012 3:16 PM

Nice info, Milo. I used to love working with 17-4PH in the machine shop.

IIRC, shrinkage of 17-4PH is also not necessarily exactly linear. In my machinist days (aerospace) I remember seeing broad thin sectioned parts warp and twist on annealing. On these kinds of parts we always left plenty of material for finish machining and surface grinding to hold high flatness tolerances.

And for trivia addicts; we built lots of wind tunnel model cylindrical "balances" that had high precision machined beams for mounting strain gages. On occasion we would guess the shrinkage from annealing wrong and end up with some undersized feature or another. We found that by selectively chroming the undersized areas we could bring the part back into tolerance without trashing it and throwing it away. I'm talking about undersized by typically < .001" requiring only a minimal application of chrome. And the chrome didn't significantly alter the material/mechanical properties of the piece.

How do you manage to come up with this stuff that brings back memories I thought were long gone?

Hooker

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#7
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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/01/2012 4:20 PM

Hi Hooker.

This post found its genesis in a private request from a PMPA member who needed to know how much to allow for shrinkage in this material. I'm their "answer man" for this sort of thing.

I decided to turn it into a knowledge retention post for "them that's doin.'"

Warp and twist is characterized as distortion. I think I have a post on that regarding quenching and tempering on here as well: 8 Reasons

Thanks for your comment.

Milo

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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/02/2012 8:28 AM

Thanks for that link, Milo. I missed that one somehow!

Hooker

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#9

Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/02/2012 4:51 PM

We are having problems with some 17-4 parts right now.

they are about 20" long, 3/8" thick and 4" wide.

We have a profile tol of .02 but there are 2 holes, one at each end that have a true pos. of .002 to each other.

the problem is, whenever we take a cut along the profile, the bar warps and twists beyond the tolerance.

I'm not sure of the heat-treat but, I they are for the oilfield industry.

Are there any tips you could give us?

I can get more inforomation on Monday.

Thanks in advance,

Calvin

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#10
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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/02/2012 4:59 PM

For that kind of profile, we used to shim them on a mill table, machine one side, turn over and shim, rinse repeat until nearly flat, then repeat the whole process on a surface grinder.

Thank God we weren't a production shop!!

Hooker

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#11
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Re: Dimensional Contraction of 17-4 PH Stainless Steel

03/02/2012 5:02 PM

Well the facts that we will surely need is the condition of the material that you are cutting. It is probably not condition A. Condition A is difficult to cut and very stringy chip issues. Condition H 900 is probably the better cutting "temper" of the 17-4 tempers available.

So we will need to know condition.

When you get the additional info send me a private message online and we can exchange emails and phone numbers and we'll see if I can help.

Milo

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