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Anonymous Poster #1

Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/10/2011 3:38 AM

Would like to know the best material applicable for the volute , impeller and shaft for pumping sulphuric acid at 98% concentration and also the shaft sealing arrangement whether double or single mechanical or any other type.

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#1

Re: Material of construction for pumping sulphuric acid at 98% concentration

09/10/2011 4:02 AM

for small volumes I would consider a vinyl transparent hose pump. Easy to maintain and to check. If maintenance is needed, just replace the hose.

For higher volumes you might think of a separate pump house and rotor in plastic of PTFE with a magnetic coupling to a motor. Some models work without shaft.

For the big work try to get a ceramic one.

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#2
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Re: Material of construction for pumping sulphuric acid at 98% concentration

09/10/2011 7:46 AM

Thanks for prompt reply.

The flow rate is around 350lph and head requirement is 24 mts water column

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#3
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Re: Material of construction for pumping sulphuric acid at 98% concentration

09/10/2011 10:33 AM

Too small flow for a centrif. This is metering pump territory. You could use a hose pump a la dvmdsc, or diaphragm type metering pump (PTFE or similar diaphragm). Maybe a small helical rotor pump if available in resistant materials.

Make sure it's adequately shielded, you don't want 98% sulphuric in somebody's face!

Codey

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#7
In reply to #2

Re: Material of construction for pumping sulphuric acid at 98% concentration

09/11/2011 1:16 AM

pneumatic pressure can also be used for batch pumping. better the air is dry.

other options is CI pumps.

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#10
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Re: Material of construction for pumping sulphuric acid at 98% concentration

09/12/2011 7:57 AM

Not vinyl! Severe effect!

http://www.coleparmer.com/techinfo/chemcomp.asp

Select "PVC" on the left and "Sulfuric acid, 75-100%" on the right to see.

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#4

Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/10/2011 3:11 PM

What is the fluid temperature? (Quite important!)

Codey is almost right. In fact, there are plenty of small plastic (& metallic) mag-drive centrifs that go down to this flowrate would be ideal for this duty (look at Iwaki, MarchMay, Totton, Speck, etc.). Unfortunately most of these only go up to 15-18m head. However, some of these, and others, also do regenerative turbine pumps (also effectively centrifs) that will do the duty.

In terms of materials, if the temperature allows, you can use PVDF, ETFE (or ETCFE), PFA linings, or PPS. If the temperature precludes plastics you will be looking at high chrome/nickel alloys, such as ferrallium (alloy 20), duplex stainless steels, or hastelloys. Mag-drive avoids seal problems.

Always use a centrif if you can (simplicity, life, cost, etc.), next diaphragm, avoid peristaltic (hose pump) if you can (says he who used to sell them!).

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#5
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Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/10/2011 9:58 PM

The temperature is ambient ie around 35 to 40 deg.C.As suggested mag-drive pumps seem to be ideal as seal problems can be avoided.

Further would like to know the indian suppliers.

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#8
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Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/11/2011 2:59 PM

Iwaki MDT series should be just right. I don't kinow if they have distributors in India, you'll have to look it up:

http://www.iwakipumps.jp/e_products/e_cascade/e_mdt.html

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#11
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Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/12/2011 1:09 PM

Indian suppliers .... here.

Sorry couldn't resist.

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#6

Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/10/2011 10:32 PM
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#9

Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/11/2011 11:30 PM

Are you referring to the seal of the vessel (I assume agitated) for the acid or the pumps? If you are referring to the vessel agitator seal, then unless you are working at high temperatures, you may use a single mechanical seal, sulphuric acid has relatively low vapor pressure, so it should be fine unless you are working in a very humid atmosphere.

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#12

Re: Material of Construction for Pumping Sulphuric Acid at 98% Concentration

09/12/2011 11:41 PM

It is good to use AODD pump u should first confirm the material of construction of the pump. it must be anti corrosive such as PTFE. and use FRL for air in line.

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